Skip to content
OpenSampling

2025 · Journal of chromatography. B, Analytical technologies in the biomedical and life sciences · paywalled

Analytical and clinical validation of a volumetric absorptive microsampling (VAMS) - Ultra performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS) method for the analysis of Clofazimine in whole blood

Nugraha et al.

The finding, in our words

VAMS finger-prick sampling showed moderate agreement with conventional venous sampling for clofazimine, with a systematic 13% lower concentration that can be corrected, and was more cost-effective by about 4.45 USD per sample, supporting its use for routine therapeutic drug monitoring in MDR-TB.

A paraphrase to the Library’s standard, never the abstract. The source is one link away and is always the authority.

Labels

  1. 2023

    Developing a Method for Quantifying Meropenem in Children-Volumetric Adsorptive Microsampling Versus Plasma Sampling

    Volumetric absorptive microsampling of whole blood did not provide a reliable basis for calculating meropenem plasma concentrations in critically ill children, so a validated low volume plasma method was required for paediatric therapeutic drug monitoring.

    Ramadan et al., Therapeutic drug monitoring (paywalled) · source ↗

    • blood
    • dried
    • vams
    • neoteryx-mitra
    • validation
    • venous-agreement
    • pediatric
    • tdm
    • antimicrobials
  2. 2022

    Comparison of conventional dried blood spots and volumetric absorptive microsampling for tacrolimus and mycophenolic acid determination

    Clinical validation for tacrolimus and mycophenolic acid monitoring showed that while volumetric absorptive microsampling met analytical criteria after concentration correction, conventional dried blood spots achieved superior adherence to strict clinical criteria, sample quality, and cost efficiency without significant haematocrit bias.

    Paniagua-González et al., Journal of pharmaceutical and biomedical analysis (paywalled) · source ↗

    • blood
    • dried
    • capillary
    • vams
    • dbs
    • neoteryx-mitra
    • self-collection
    • validation
    • venous-agreement
    • tdm
    • immunosuppressants
    • economics
    • haematocrit
  3. 2021

    Development and validation of an LC-MS/MS method for the quantification of the anthelmintic drug moxidectin in a volumetric absorptive microsample, blood, and plasma: Application to a pharmacokinetic study of adults infected with Strongyloides stercoralis in Laos

    The study developed and validated an LC-MS/MS method for moxidectin and showed that capillary Mitra® microsampling in Strongyloides-infected adults yielded pharmacokinetic profiles in close agreement with venous sampling, with identical time to maximal concentration of 4.0 hours and similar maximal concentrations of 83.9–88.5 ng/mL. This demonstrates the method and device are suitable for therapeutic drug monitoring of anthelmintics in decentralised field settings.

    Hofmann et al., Journal of chromatography. B, Analytical technologies in the biomedical and life sciences (paywalled) · source ↗

    • vams
    • venous-agreement
    • neoteryx-mitra
    • blood
    • tdm
    • haematocrit
    • dried
    • antimicrobials
    • capillary
    • validation
  4. 2019

    Pharmacokinetics of Albendazole, Albendazole Sulfoxide, and Albendazole Sulfone Determined from Plasma, Blood, Dried-Blood Spots, and Mitra Samples of Hookworm-Infected Adolescents

    The validated LC-MS/MS method showed similar pharmacokinetic profiles for albendazole and its metabolites across plasma, whole blood, dried blood spots and Mitra microsamples from hookworm-infected adolescents, supporting microsampling for paediatric pharmacokinetic studies. Mitra extraction proved more robust than dried blood spots during validation and is recommended for future albendazole pharmacokinetic work, despite higher albendazole sulfone concentrations observed in both microsampling devices compared with wet matrices.

    Schulz et al., Antimicrobial agents and chemotherapy (paywalled) · source ↗

    • blood
    • liquid
    • dried
    • capillary
    • vams
    • dbs
    • neoteryx-mitra
    • validation
    • venous-agreement
    • pediatric
    • tdm
    • antimicrobials
  5. 2026

    Evaluation of hematocrit-adjusted conversion strategies for mycophenolic acid and tacrolimus monitoring using volumetric absorptive microsampling in lung and renal transplant recipients

    In lung and renal transplant recipients, VAMS sampling with LC-MS/MS quantification of mycophenolic acid and tacrolimus showed good linearity and accuracy, and with a haematocrit-adjusted conversion formula achieved clinical agreement in most samples; tacrolimus did not require haematocrit correction. The approach is virtually painless and enables richer sampling for more accurate drug exposure estimates, supporting decentralised therapeutic drug monitoring.

    Juan et al., Journal of pharmacy & pharmaceutical sciences : a publication of the Canadian Society for Pharmaceutical Sciences, Societe canadienne des sciences pharmaceutiques · source ↗

    • blood
    • dried
    • vams
    • neoteryx-mitra
    • validation
    • venous-agreement
    • tdm
    • immunosuppressants
    • haematocrit