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OpenSampling

2022 · The Analyst · paywalled

In-depth evaluation of automated non-contact reflectance-based hematocrit prediction of dried blood spots

Boffel et al.

The finding, in our words

The authors validated a quadratic calibration model for automated UV-Vis-based haematocrit prediction from dried blood spots, achieving bias below 0.025 L L-1 and total precision of 2.7%. In therapeutic drug monitoring of tacrolimus, predicted haematocrit values showed good concordance with reference Sysmex measurements, supporting the use of this patient-centric microsampling approach for decentralised immunosuppressant monitoring.

A paraphrase to the Library’s standard, never the abstract. The source is one link away and is always the authority.

Labels

  1. 2023

    Automated dried blood spot analysis achieved clinical and analytical acceptance criteria for tacrolimus, sirolimus, everolimus and cyclosporin A after haematocrit correction. This validates a method that could enable decentralised, patient-centric therapeutic drug monitoring for transplant recipients.

    Application of a Fully Automated Dried Blood Spot Method for Therapeutic Drug Monitoring of Immunosuppressants: Another Step Toward Implementation of Dried Blood Spot AnalysisDeprez & Stove, Archives of pathology & laboratory medicine (paywalled) · source ↗

    • blood
    • dried
    • dbs
    • validation
    • venous-agreement
    • tdm
    • immunosuppressants
    • haematocrit
  2. 2022

    Clinical validation for tacrolimus and mycophenolic acid monitoring showed that while volumetric absorptive microsampling met analytical criteria after concentration correction, conventional dried blood spots achieved superior adherence to strict clinical criteria, sample quality, and cost efficiency without significant haematocrit bias.

    Comparison of conventional dried blood spots and volumetric absorptive microsampling for tacrolimus and mycophenolic acid determinationPaniagua-González et al., Journal of pharmaceutical and biomedical analysis (paywalled) · source ↗

    • blood
    • dried
    • capillary
    • vams
    • dbs
    • neoteryx-mitra
    • self-collection
    • validation
    • venous-agreement
    • tdm
    • immunosuppressants
    • economics
    • haematocrit
  3. 2022

    A new LC-MS/MS method quantifies four immunosuppressants from one 3.2 mm dried blood spot using cold-induced phase separation, achieving accurate results and favourable interchangeability with a certified whole blood method in 120 paired clinical samples, supporting decentralised therapeutic drug monitoring.

    Quantification of immunosuppressants from one 3.2 mm dried blood spot by a novel cold-induced phase separation based LC-MS/MS methodLe et al., Analytica chimica acta (paywalled) · source ↗

    • venous-agreement
    • blood
    • dbs
    • tdm
    • haematocrit
    • dried
    • immunosuppressants
    • validation
  4. 2017

    The study validated a dried blood spot assay for five immunosuppressants on two LC-MS/MS systems, showing that haematocrit effects stayed within 15% across a clinically relevant range (0.23–0.48 l/l) without correction. Clinical validation confirmed that tacrolimus and cyclosporin A results from dried blood spots matched those from conventional whole blood, supporting home-based therapeutic drug monitoring without haematocrit adjustment.

    Dried blood spot validation of five immunosuppressants, without hematocrit correction, on two LC-MS/MS systemsKoster et al., Bioanalysis (paywalled) · source ↗

    • blood
    • dried
    • dbs
    • self-collection
    • validation
    • venous-agreement
    • tdm
    • immunosuppressants
    • haematocrit
  5. 2026

    In AML and CLL, 91% of VAMS venetoclax results fell within 20% of plasma after individualised haematocrit correction; in home sampling, 18 of 21 patients self-sampled independently and 76% of returned samples were analysable, which shows home microsampling is workable, though the authors ask for multicentre validation.

    Clinical Validation of Venetoclax Volumetric Microsampling in Leukemia, with Whole-Blood-to-Plasma Conversion and Self-Microsampling FeasibilityLevens et al., Clinical Pharmacokinetics (paywalled) · source ↗

    • vams
    • venous-agreement
    • blood
    • dbs
    • tdm
    • self-collection
    • haematocrit
    • dried
    • oncology
    • capillary
    • validation