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OpenSampling

2026 · Journal of analytical toxicology · open access

Validation of a microsampling-compatible liquid-liquid extraction method for cannabinoid quantitation in 50 µL of whole blood using liquid chromatography-mass spectrometry

Mohammed et al.

The finding, in our words

The authors validated a liquid-liquid extraction LC-MS/MS method that quantifies cannabinoids in only 50 µL of liquid whole blood with lower limits of quantitation from 0.10 to 1.0 ng/mL. This microsampling approach enables roadside collection via finger prick, allowing measurement of THC levels at the time of driving without trained phlebotomists, thus overcoming delays that reduce THC concentrations.

A paraphrase to the Library’s standard, never the abstract. The source is one link away and is always the authority.

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  1. 2026

    Liquid Chromatographic Methods for Microsampling in Sports Drug Monitoring: Progress in DBS and VAMS

    The analysis indicates that dried blood spots and volumetric absorptive microsampling enable minimally invasive monitoring of prohibited substances, with volumetric absorptive microsampling offering improved quantitative reliability over traditional dried spots.

    Zhang, Biomedical chromatography : BMC (paywalled) · source ↗

    • vams
    • doping
    • blood
    • dbs
    • dried
    • steroids
    • toxicology
    • hormones
    • validation
    • biomarkers
  2. 2026

    Volumetric absorptive microsampling for profiling of signaling lipids: a comparative analysis with whole blood and dried blood spots

    Volumetric absorptive microsampling showed better precision than dried blood spots and a metabolic profile closer to whole blood, with stable signalling lipids for 24 hours at room temperature but significant changes after one week unless stabilised, indicating feasibility for decentralised sampling with the need for storage strategies.

    Thangavelu et al., Analytical and bioanalytical chemistry · source ↗

    • vams
    • volumetric
    • blood
    • dbs
    • metabolome
    • dried
    • liquid
    • validation
    • biomarkers
  3. 2026

    Application of volumetric absorptive microsampling (VAMS) for the simultaneous determination of cadmium and lead in blood

    VAMS gave near‑quantitative recovery for cadmium and lead in human blood and correlated strongly with venous sampling, with pre‑cleaning improving correlation and lowering background lead, supporting its use for decentralised biomonitoring of these toxic elements.

    Gutknecht et al., Environmental monitoring and assessment (paywalled) · source ↗

    • vams
    • venous-agreement
    • blood
    • dried
    • toxicology
    • validation
  4. 2026

    Ultrasensitive de novo Protein Sandwich Lateral flow Fluorescence Assay for Cortisol in Saliva and Serum using Quantum dots and Europium Nanoparticles

    This study validated a lateral flow fluorescence assay using quantum dots for saliva and europium nanoparticles for serum to detect cortisol within physiological ranges. The test operates in 15 minutes with a handheld reader, supporting point-of-care and at-home monitoring without a cold chain.

    Bruno et al., Journal of fluorescence (paywalled) · source ↗

    • blood
    • saliva
    • liquid
    • self-collection
    • validation
    • hormones
    • cortisol
  5. 2026

    From Home to Transcriptome: Comparing the Transcriptomic Profile of Induced Immune Response via Lipopolysaccharide Stimulation in homeRNA and Venous Blood

    The homeRNA capillary blood collection and stabilization platform successfully captured lipopolysaccharide-induced inflammatory gene expression profiles. These transcriptomic responses were comparable to those obtained from traditional venous blood samples stabilized with RNAlater or PAXgene, demonstrating the platform's suitability for remote transcriptomic monitoring.

    Brown et al., Analytical chemistry (paywalled) · source ↗

    • venous-agreement
    • stabilised
    • blood
    • capillary
    • liquid
    • validation
    • biomarkers